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Thermal stability and decomposition mechanisms of …

The C 3 A was mechanically mixed with reagent grade gypsum, CaSO 4 ·2H 2 O, in the ratio 0.02 mol to 0.06 mol. The powder was slurried into 1 L of distilled decarbonated water …

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Thermal analysis of calcium sulfate dihydrate sources used …

Gypsum wallboard has been used for over 100 years as a barrier to the spread of fire in residential and commercial structures. The gypsum molecule, CaSO 4 ·2H 2 O, provides …

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Gypsum content determination in Portland cements by thermogravimetry

Figure 1 shows the TG and DTG curves of a high-purity gypsum sample. As thermal decomposition is occurring in an open pan, the steps represented by Eqs. 2 and 3 occur …

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(PDF) Lightweight composite gypsum boards …

The current strategy for developing fire-resistant gypsum boards is mainly based on adding porous materials. However, these additives are generally weaker in strength due to higher porosity and ...

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APPLICATION OF GYPSUM BOARD TO FORM CURVED …

A stop shall be applied at one end of the curve to restrain one end or edge of the gypsum board during installation. Pressure shall be applied to the unrestrained end or edge of the gypsum …

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Thermal Analysis | Construction Materials Consultants, Inc.

120, 180-200°C = Gypsum decomposition and water release (endotherm) 100-200ºC = Hydrate water from decomposition of calcium silicate hydrate (CSH) ... hence did not show noticeable …

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Thermal Analysis of Gypsum

transition from hemihydrate gypsum to crystalline gypsum (dihydrate gypsum). This brief presents examples of TG/DTA and DSC measurements of the thermal changes of gypsum.

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Thermal Analysis & Rheology THERMAL SOLUTIONS

percent gypsum in stucco. This curve is prepared by characterizing (using the pinhole pan procedure) a series of reference materials prepared to cover the anticipated range of the test …

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Overlay of gypsum DSC curves obtained with open crucibles in …

Figure 2 shows an overlay of gypsum DSC curves obtained with open crucibles in STA at atmospheric pres- sure and in DSC at 1, 16, 34, 50, and 67 bar. ... The weight loss owing to …

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Speciation of mercury in FGD gypsum and mercury emission …

The thermal decomposition curves obtained from the Hg reference samples, including HgCl 2, Hg 2 Cl 2, HgS, HgO, HgSO 4, and Hg 2 SO 4, are shown in Fig. 2. ... For …

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Novel approach to thermal degradation kinetics of gypsum: application

In this work, we have reinvestigated the thermal degradation kinetics of synthetic gypsum (CaSO4·2H2O) using a novel approach based on peak deconvolution followed by the …

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Fate of mercury in flue gas desulfurization gypsum …

The Hg release curves (Hg t) generated by thermal decomposition of the seven FGD gypsum samples are shown in Fig. 4. By integrating the peak area of each Hg release …

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Changes in structure and composition of gypsum paste at …

The DSC curve of gypsum powder showed an endothermic peak at the temperature 180 °C, which corresponded to the dehydration of bassanite to anhydrite. ... The …

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(PDF) The thermal dehydration of natural …

The DSC curve for the dehydration of calcium sulphate dihydrate shows a double peak which was not present in the DSC curve for the dehydration of natural gypsum. The mean weight loss for calcium sulphate dihydrate was …

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The use of thermogravimetric analysis …

Fig. 6 TG and DTG curves for the decomposition of the dihydrate using 100 mL sealed aluminium pan: a – 20°C min–1 ; b – 10°C min–1 heating rate (sample mass: 25 mg) Table 3 Regression parameters from Kissinger equation for …

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Gypsum plaster waste recycling: A potential environmental …

2015. The feasibility of incorporation of recycled gypsum derived from post-consumer (construction and demolition) gypsum-based waste into the plasterboard manufacturing …

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Thermogravimetric Study of Dehydration and Thermal …

Fig. 1. Example of TGA mass and mass loss rate curves (Type C gypsum board heated at 20 °C/min). ARRHENIUS-RATE THERMAL DECOMPOSITION KINETICS . Consider an …

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Study on Kinetic Parameters and Reductive Decomposition …

3.1 Thermo Composition Process of Gypsum. TG and DTA curves of AG, DG and WG gypsum are shown in Fig. 1.The thermal decomposition process of AG can be separated …

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Partitioning effect of mercury content and speciation in gypsum …

Additionally, a comparison of the mercury present in WFGD gypsum from five different coal-fired power plants using thermal decomposition techniques showed that the …

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Thermal Analysis of Calcium Sulfate Dihydrate Sources Used …

This explains the decomposition of gypsum at different forms of calcium sulphate dihydrate (CaSO 4 ·2H 2 O) to calcium sulphate anhydrite (CaSO 4 ) between 85 to 400 • C …

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Curves of the thermogravimetric analysis (TGA) of …

Studies suggest that the peak in the specific curve around 700-800 °C corresponds to the decomposition of the calcium carbonate and magnesium carbonate content of the gypsum boards, and...

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of Gypsum by Carbon Monoxide

For this study natural gypsum having the following composition was used. The gypsum was crushed and then sep- arated by Tyler standard sieves into narrow-size fractions. The -7f8 …

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Clinker-Free Cement: A New Reality

Figure 5 and Figure 6 show the thermogravimetric curves of the cement mixture pastes after 3, 7, ... After 28 days of curing, characteristic peaks of gypsum decomposition …

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Recycling of pyrite and gypsum mining residues through …

DTA curve shows two close endothermic peaks in the temperature range 120–200 °C as an indication of gypsum dehydration (Engbrecht and Hirschfeld, 2016) as well as a …

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Structural evolution of gypsum (CaSO4·2H2O) during …

Two–step process in the dehydration of gypsum Supplementary Figure S1 (Fig. S1–S4 are available on-line from https://doi/10.2465/jmps.220811) shows the TG and DTA curves of …

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Utilization of Desulfurization Gypsum to Producing SO …

decomposition of gypsum under different reducing atmo-sphere was carried out in the PTGA, Thermax 500. The gypsum used in the experiment is phosphogypsum, which ... Fig. 2 …

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TG/DSC and thermal expansion curves of pure gypsum …

Figure 1 shows the TG/DSC and thermal expansion curves of the gypsum between 20 and 800 C. The TG/DSC curves reveal that the bound water in CaSO 4 ·2H 2 O was totally removed …

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2: Thermogravimetry

Decomposition curve for a mixture of calcium and magnesium oxalate dihydrate. There is a significant loss which occurs before 210°C- due to loss of water from the sample. ... So, if there is conversion of gypsum to …

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Partitioning effect of mercury content and speciation in gypsum …

The relationship between separation time and the Hg compounds in gypsum. The thermal decomposition curves of Hg compounds in the FGD gypsum are shown in Fig. 8. After …

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Application: TGA PT 1600 – Gypsum plaster decomposition

The measurement shows that the carbon and organic content of the "bad" samples (green and blue curves) is almost identical with the reference samples (red and black curve). The weight …

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